Procedure:
- Select the weight of aspirin from the slider.
- Click on the “Add aspirin button†to take aspirin in the R.B flask.
- Click on the “Add NaOH†button to add 40 mL 10% NaOH.
- Click on the “Nextâ€ÂÂ.
- Click on the “Reflux†button to reflex the content for 15 minutes.
- Click “Nextâ€ÂÂ.
- Click “Transfer solution†button to transfer it into 250 mL standard flask.
- Click “Make up solution†button to make up the solution upto the mark.
- Click “Nextâ€ÂÂ.
- Select the volume of aspirin.
- Click “Pipette out†button to pipette out the aspirin.
- Click on the “box†in front of ‘Preparation of titrate’ we can see procedure of preparation of titrate (aspirin) after selecting the volume of aspirin.
- Click “Nextâ€ÂÂ.
- Select the titrant (sodium thiosulphate).
- Adjust the speed of drops.
- Click on the “Start†button to start titration.
- Near the end point the colour just fades, then click on “Add Starch†button to add indicator.
- Adjust the speed of drops.
- Click on “Start†button to continue the titration.
- When blue colour disappears click on the “stop†button to stop the titration .
Note:- Here 50 mL brominating mixture (Blank) = 45.6 mL thiosulphate.